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(ii) Fumaric acid-grafted polyethylene (CAS Reg. No. 26877-81-6) consists of basic polymers manufactured by the catalytic polymerization of ethylene followed by reaction with fumaric acid in the absence of free radical initiators. Such polymers shall contain grafted fumaric acid at levels not to exceed 2 percent by weight of the finished polymer.
(vi) Olefin basic copolymers (CAS Reg. No. 61615-63-2) manufactured by the catalytic copolymerization of ethylene and propylene with 1,4-hexadiene, followed by reaction with fumaric acid in the absence of free radical initiators. Such polymers shall contain not more than 4.5 percent of polymer units deriving from 1,4-hexadiene by weight of total polymer prior to reaction with fumaric acid and not more than 2.2 percent of grafted fumaric acid by weight of the finished polymer.
(b ) Evaporating apparatus. Rapid evaporation of large volumes of solvent requires special precautions to prevent contamination by dust. This is facilitated by a special "gas" cover consisting of an inverted flat Pyrex crystallizing dish of an appropriate size (190 millimeters * 100 millimeters) to fit a 1-liter beaker. Through the center of the dish are sealed an inlet tube for preheated, oxygen-free nitrogen, and an outlet tube located 1 inch off center. Nitrogen is fed from the supply source through a coil of 1/4-inch stainless steel tubing immersed in the same steam bath used to supply heat for solvent evaporation. All connections are made with flexible tetrafluoroethylene tubing.
(f ) Sample basket (Optional). A perforated stainless steel cylindrical basket that is approximately 1.5 inches in diameter, 1.6 inches high, and has perforations of 0.125 inches in diameter for 33 holes/in2, or 40 percent open area. The basket should pass freely through the 45/50 female joint of the extraction flask. A No. 6-32 stainless steel eye-bolt is attached to the lid for positioning the basket in the extraction vessel. The positioning rod, approximately 18 inches long and made from 1/16 inch outside diameter 316 stainless steel welding rod or equivalent and hooked at both ends, is used to position the basket in the extraction apparatus.
(h ) Reagents. n -Hexane, reagent or spectrograde, aromatic free (less than 1 milligram per liter), minimum 85 percent n -hexane. This reagent may be reused until it contains a maximum of 1.5 grams polyolefin extractables or has been used for 12 determinations.
(4) Maximum soluble fraction in xylene - (i) Olefin copolymers described in paragraph (a )(3 )(ii ) of this section, polypropylene, and poly (methylpen-tene ). A sample is dissolved completely in xylene by heating and stirring in a bottle with little free space. The solution is allowed to cool without stirring, whereupon the insoluble portion precipitates and is filtered off; the total solids content of the filtrate is then determined as a measure of the soluble fraction.
(c ) Procedure. Transfer 5 grams +/-0.001 gram of sample to the resin kettle, add 1,000 milliliters (840 grams) of xylene, and clamp top in position after inserting a piece of glass rod to prevent bumping during reflux. Start water flowing through the jacket of the reflux condenser and apply full voltage (115 volts) to the heating mantle. When the xylene starts to boil, reduce the voltage to a level just sufficient to maintain reflux. After refluxing for at least 2 hours, disconnect the power source to the mantle, remove the kettle, and allow to cool in air until the temperature of the contents drops to 50 deg.C, after which the kettle may be rapidly cooled to 25 deg.C-30 deg.C by immersing in a cold water bath. Transfer the kettle to a constant temperature bath set to maintain 25 deg.C +/-0.1 deg.C, and allow to equilibrate for a least 1 hour (may be left overnight if convenient). Break up any precipitated polymers that may have formed, and decant the xylene solution successively through a fast filter paper and then through a fritted-glass filter into a tared 1-liter Erlenmeyer flask, collecting only the first 450 milliliters - 500 milliliters of filtrate (any attempt to collect more of the xylene solution usually results in clogging the filter and risking losses). Reweigh the Erlenmeyer flask and calculate the weight of the filtrate obtained to the nearest 0.1 gram. Transfer the filtrate, quantitatively, from the Erlenmeyer flask to the 1-liter beaker, insert the beaker in its heating mantle, add a glass-coated magnetic stirring bar, and mount the gas cover in place, connecting the inlet tube to the nitrogen source and the outlet to the condenser of the receiving flask. Start a flow of nitrogen (2 to 3 liters per minute) into the gas cover and connect an aspirator to the receiver using a free-flow rate equivalent to 6-7 liters of air per minute. With the infrared lamp on, adjust the voltage to the heating mantle to give a distillation rate of 12-13 milliliters per minute when the magnetic stirrer is revolving just fast enough to promote good boiling. When the volume of solvent in the beaker has been reduced to 30-50 milliliters, transfer the concentrated extractive to a suitable weighing dish that has been previously tared (dry). Rinse the beaker twice with 10-20 milliliter portions of fresh xylene, adding the rinsings to the weighing dish. Evaporate the remainder of the xylene on an electric hotplate set at low heat under the gas cover with a stream of nitrogen directed toward the center of the dish. Avoid any charring of the residue. Transfer the weighing dish to a vacuum desiccator at room temperature and allow to remain under reduced pressure for at least 12 hours (overnight), after which determine the net weight of the residue to the nearest 0.0001 gram. Correct the result for nonvolatile solvent blank obtained by evaporating the equivalent amount of xylene under identical conditions. Calculate the weight of residue originally present in the total weight of solvent (840 grams), using the appropriate factor based on the weight of filtrate evaporated.
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The Amazon API Gateway free tier includes one million API calls received for REST APIs, one million API calls received for HTTP APIs, and one million messages and 750,000 connection minutes for WebSocket APIs per month for up to 12 months. If you exceed this number of calls per month, you will be charged the API Gateway usage rates.
These free tier offers are only available to new AWS customers, and are available for 12 months following your AWS sign-up date. When your 12 month free usage term expires or if your application use exceeds the tiers, you simply pay standard, pay-as-you-go service rates.
Pay only for the API calls you receive and the amount of data transferred out. There are no data transfer out charges for Private APIs. However, AWS PrivateLink charges apply when using Private APIs in API Gateway. API Gateway also provides optional data caching charged at an hourly rate that varies based on the cache size you select. For REST APIs, the API Gateway free tier includes one million API calls per month for up to 12 months.
Each file can also have a maximum size specified. If a maximum size isn't specified, the file can continue to grow until it has used all available space on the disk. This feature is especially useful when SQL Server is used as a database embedded in an application where the user doesn't have convenient access to a system administrator. The user can let the files autogrow as required to reduce the administrative burden of monitoring free space in the database and manually allocating additional space.
Filegroups use a proportional fill strategy across all the files within each filegroup. As data is written to the filegroup, the SQL Server Database Engine writes an amount proportional to the free space in the file to each file within the filegroup, instead of writing all the data to the first file until full. It then writes to the next file. For example, if file f1 has 100 MB free and file f2 has 200 MB free, one extent is given from file f1, two extents from file f2, and so on. In this way, both files become full at about the same time, and simple striping is achieved. 2ff7e9595c
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